Rapid microwave sintering of centimetric zirconia: Scalability and electromagnetic‐thermal‐fluid‐dynamic simulation
نویسندگان
چکیده
Microwave sintering is a method presenting the following advantages for flash sintering: contactless/volumetric heating, and possibility to control heating cycle of microwave power. In this study, transition from typical 100 K/min an ultra-rapid rate 500 studied. The homogeneity hybrid configuration using silicon carbide susceptors tested up stability limit system. We show that zirconia specimens as thick 10 mm can be heated sintered at which thermal cracks appear. However, centimetric size seems favor coarsening implying important remaining porosity in end. A comprehensive simulation including convection has allowed determination regime during process quantification each specimen's cooling fluxes.
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ژورنال
عنوان ژورنال: Journal of the American Ceramic Society
سال: 2022
ISSN: ['0002-7820', '1551-2916']
DOI: https://doi.org/10.1111/jace.18787